SPME Application Note Index
Solid Phase Micro Extraction
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| Note# |
Author |
Title/Description |
| 19 |
Penton |
Comparison
of Static Headspace and Headspace SPME for Determining EPA
5021 Volatiles in Water
Key Words: SPME, EPA 5021 |
| 18 |
Sergio PUCCI, Alessandro SABA, Andrea
RAFFAELLI and Piero SALVADORI |
Determination
of Phenol Content in Fibers of Industrial Interest
Key Words: SPME, Fibers |
| 17 |
Penton |
Quantitative
Determination of Vinyl Chloride in a Polymer with Automated
SPME
Key Words: SPME, Vinyl Chloride, Polymers |
| 16 |
Penton |
Determining
Sulfur Volatiles in Beer w/Automated SPME and PFPD Detection
Key Words: SPME, 8200CX, Food, PFPD, Sulfur |
| 15 |
Penton |
Determining
Volatiles in Beer w/Automated SPME and GC/MS/ECD
Key Words: SPME, 8200CX, Food, Saturn |
| 14 |
Magdic, Pawliszyn |
Analysis
of Acetone and C1 - C4 Alcohols using Automated SPME
Key Words: SPME, 8200CX, Alcohol, Beverages |
| 13 |
Penton |
Screening
Packaging Materials with Automated SPME and GC/MS
Key Words: SPME, 8200CX, Polymers, Saturn |
| 12 |
Penton |
Performance
of Automated SPME: A Comparison of Results with an Interlaboratory
GC/MS Pesticide Study
Key Words: SPME, 8200CX, Pesticides, Saturn |
| 11 |
Penton |
Determination
of Phenols in Water with automated SPME and Agitation
Key Words: SPME, 8200CX, Blood, Phenols |
| 10 |
Jennison and Jennison |
Rapid
Analysis of BTEX and TPH in Water using Solid Phase Microextraction
(SPME) and FastGC
Key Words: FastGC, SPME, 8200CX, BTEX |
| 9 |
Penton |
Blood
Alcohol Determination with Automated Solid Phase Microextraction
(SPME): A Comparison with Static Headspace
Key Words: SPME, 8200CX, Blood, Alcohol |
| 8 |
Penton |
Determination
of Trace Methanol in a Caustic Industrial Product with Automated
Solid Phase Microextraction (SPME)
Key Words: SPME, 8200 AutoSampler, Methanol, Industrial Applications |
| 7 |
Penton |
Determination
of Residual Solvents and Monomers in Polymers with Solid
Phase Microextraction (SPME) and GC/MS
Key Words: SPME, 8200 AutoSampler, Polymers, GC/MS |
| 6 |
Penton |
Characterization
of Flavor Components in Wines with SPME, GC and GC/MS
Key Words: SPME, 8200 AutoSampler, Wine, Foods & Flavors, GC/MS |
| 5 |
Penton |
Analysis
of Therminol in Water using Solid Phase Microextraction
Key Words: SPME, Therminol, Biphenyl, Diphenyl Oxide, Water |
| 4 |
Penton |
Flavor
Analysis of a Fruit Beverage with Automated Solid Phase Microextraction
Key Words: SPME, 8200 AutoSampler, Foods and Flavors |
| 3 |
Penton |
Determination
of a Wide Range of Organic Impurities in Water with Automated
Solid Phase Microextraction
Key Words: SPME, 8200 AutoSampler, Volatiles, Semivolatiles |
| 2 |
Penton |
Determination
of Residual Solvents in Pharmaceuticals with Automated Solid
Phase Microextraction
Key Words: SPME, 8200 AutoSampler, Beverages, Food
Description: This note describes the use of solid phase
microextraction (SPME) for determining organic volatile impurities
in pharmaceutical compounds.
In addition to the solvents listed in the United States Pharmacopeia
(USP) National Formulary, several additional solvents were
considered to conform
to compounds actually used in pharmaceutical companies. These were ethanol,
acetone, isopropanol and toluene. The results, which included a recovery
study on two pharmaceutical compounds, indicated that SPME easily met
the precision and sensitivity requirements of the USP and
is a good alternative
to liquid injection or static headspace. An automated SPME system is
considerably less expensive and far more compact than a dedicated
static headspace system,
and the problems of injecting aqueous samples into a GC are avoided. |
| 1 |
Penton |
Profiling
Flavors in Alcoholic and Non-Alcoholic Beverages with Automated
SPME
Key Words: SPME, 8200 AutoSampler, Beverages Food
Description: Flavors in foods and beverages are monitored
by static headspace GC and occassionally by thermal desorption
or purge and trap. The result
is a "fingerprint" chromatogram that can be examined to determine
if the particular sample meets the standards set by the manufacturer, or
if components are present that might adversely affect the taste of the
product. Solid Phase Microextraction (SPME), a new technique for introducing
analytes into a GC, is used in this application. The note illustrates that
SPME is suitable for "fingerprinting" foods and flavors, and
offers several advantages over competing techniques. |
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